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Synthesis and crystallographic study of Pb-Sr hydroxyapatite solid solutions by high temperature mixing method under hydrothermal conditions
http://hdl.handle.net/10126/4680
http://hdl.handle.net/10126/468064509aba-4ba8-40ef-ba44-9e90a485fdaf
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
MRB-08-260R1-revised manuscript[1].pdf (1.8 MB)
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| Item type | 学術雑誌論文 / Journal Article(1) | |||||
|---|---|---|---|---|---|---|
| 公開日 | 2010-08-06 | |||||
| タイトル | ||||||
| タイトル | Synthesis and crystallographic study of Pb-Sr hydroxyapatite solid solutions by high temperature mixing method under hydrothermal conditions | |||||
| 言語 | en | |||||
| 言語 | ||||||
| 言語 | eng | |||||
| キーワード | ||||||
| 言語 | en | |||||
| 主題Scheme | Other | |||||
| 主題 | Pb-Sr hydroxyapatite | |||||
| キーワード | ||||||
| 言語 | en | |||||
| 主題Scheme | Other | |||||
| 主題 | Chemical synthesis | |||||
| キーワード | ||||||
| 言語 | en | |||||
| 主題Scheme | Other | |||||
| 主題 | X-ray diffraction | |||||
| キーワード | ||||||
| 言語 | en | |||||
| 主題Scheme | Other | |||||
| 主題 | Crystal structure | |||||
| 資源タイプ | ||||||
| 資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
| 資源タイプ | journal article | |||||
| 著者 |
Zhu, Kongjun
× Zhu, Kongjun× Yanagisawa, Kazumichi× Shimanouchi, Rie× Onda, Ayumu× Kajiyoshi, Koji× Qiu, Jinhao |
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| 抄録 | ||||||
| 内容記述タイプ | Abstract | |||||
| 内容記述 | The solid solutions in the system of Pb and Sr hydroxyapatite, Sr10-xPbxHAp (x= 0-10), were successfully synthesized by high-temperature mixing method (HTMM) at 160ºC for 12 hours under hydrothermal conditions. The samples were characterized by X-ray diffraction, chemical analysis and electron microscopic observation, and the site of the metal ions in the solid solutions was analyzed with the Rietveld method. The lattice constants, both a and c, of the solid solutions varied linearly with Pb content. It was found that Pb ions in the solid solutions preferentially occupied the M (2) site in the apatite structure. HTMM gives Sr-Pb HAp solid solutions much better crystallization. However, due to the formation of intermediate compound of Pb3O2(OH)2 in the Pb(NO3)2•4H2O solution before mixing with (NH4)2HPO4 solution at 160°C, HTMM causes the decrease of crystallization of the samples with high Pb content. | |||||
| 書誌情報 |
en : Materials research bulletin : an international journal reporting research on crystal growth and materials preparation and characterization 巻 44, 号 6, p. 1392-1396, 発行日 2009 |
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| ISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 00255408 | |||||
| 書誌レコードID | ||||||
| 収録物識別子タイプ | NCID | |||||
| 収録物識別子 | AA00722973 | |||||
| フォーマット | ||||||
| 内容記述タイプ | Other | |||||
| 内容記述 | application/pdf | |||||
| 出版者 | ||||||
| 出版者 | Elsevier | |||||
