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  1. 理工学
  2. 学術論文

Synthesis and crystallographic study of Pb-Sr hydroxyapatite solid solutions by high temperature mixing method under hydrothermal conditions

http://hdl.handle.net/10126/4680
http://hdl.handle.net/10126/4680
64509aba-4ba8-40ef-ba44-9e90a485fdaf
名前 / ファイル ライセンス アクション
MRB-08-260R1-revised MRB-08-260R1-revised manuscript[1].pdf (1.8 MB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2010-08-06
タイトル
タイトル Synthesis and crystallographic study of Pb-Sr hydroxyapatite solid solutions by high temperature mixing method under hydrothermal conditions
言語 en
言語
言語 eng
キーワード
言語 en
主題Scheme Other
主題 Pb-Sr hydroxyapatite
キーワード
言語 en
主題Scheme Other
主題 Chemical synthesis
キーワード
言語 en
主題Scheme Other
主題 X-ray diffraction
キーワード
言語 en
主題Scheme Other
主題 Crystal structure
資源タイプ
資源タイプ識別子 http://purl.org/coar/resource_type/c_6501
資源タイプ journal article
著者 Zhu, Kongjun

× Zhu, Kongjun

10262

Zhu, Kongjun

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Yanagisawa, Kazumichi

× Yanagisawa, Kazumichi

10263

Yanagisawa, Kazumichi

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Shimanouchi, Rie

× Shimanouchi, Rie

10264

Shimanouchi, Rie

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Onda, Ayumu

× Onda, Ayumu

10265

Onda, Ayumu

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Kajiyoshi, Koji

× Kajiyoshi, Koji

10266

Kajiyoshi, Koji

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Qiu, Jinhao

× Qiu, Jinhao

10267

Qiu, Jinhao

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抄録
内容記述タイプ Abstract
内容記述 The solid solutions in the system of Pb and Sr hydroxyapatite, Sr10-xPbxHAp (x= 0-10), were successfully synthesized by high-temperature mixing method (HTMM) at 160ºC for 12 hours under hydrothermal conditions. The samples were characterized by X-ray diffraction, chemical analysis and electron microscopic observation, and the site of the metal ions in the solid solutions was analyzed with the Rietveld method. The lattice constants, both a and c, of the solid solutions varied linearly with Pb content. It was found that Pb ions in the solid solutions preferentially occupied the M (2) site in the apatite structure. HTMM gives Sr-Pb HAp solid solutions much better crystallization. However, due to the formation of intermediate compound of Pb3O2(OH)2 in the Pb(NO3)2•4H2O solution before mixing with (NH4)2HPO4 solution at 160°C, HTMM causes the decrease of crystallization of the samples with high Pb content.
書誌情報 en : Materials research bulletin : an international journal reporting research on crystal growth and materials preparation and characterization

巻 44, 号 6, p. 1392-1396, 発行日 2009
ISSN
収録物識別子タイプ ISSN
収録物識別子 00255408
書誌レコードID
収録物識別子タイプ NCID
収録物識別子 AA00722973
フォーマット
内容記述タイプ Other
内容記述 application/pdf
出版者
出版者 Elsevier
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Cite as

Zhu, Kongjun, Yanagisawa, Kazumichi, Shimanouchi, Rie, Onda, Ayumu, Kajiyoshi, Koji, Qiu, Jinhao, 2009, Synthesis and crystallographic study of Pb-Sr hydroxyapatite solid solutions by high temperature mixing method under hydrothermal conditions: Elsevier, 1392–1396 p.

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